Casula, M.F., Loche, D., Marras, S., Paschina, G., Corrias, A. (2007) Role of urea in the preparation of highly porous nanocomposite aerogels. Langmuir, 23 (7). pp. 3509-3512. ISSN 0743-7463. (doi:10.1021/la0635799) (The full text of this publication is not currently available from this repository. You may be able to access a copy if URLs are provided) (KAR id:46175)
| The full text of this publication is not currently available from this repository. You may be able to access a copy if URLs are provided. | |
| Official URL: http://dx.doi.org/10.1021/la0635799 |
|
Abstract
The preparation of highly porous CoFe2O4-SiO 2 nanocomposite aerogels was successfully achieved by a novel sol-gel procedure involving urea-assisted co-gelation of the precursor phases. This method allows fast gelation, giving rise to an aerogel with 97% porosity. The formation of CoFe2O4 nanocrystals homogeneously distributed within the matrix occurs after calcination at 750°C and is complete at 900°C. Despite the high temperature required for the formation of the CoFe2O4 nanocrystals, the high porosity typical of aerogels is still retained.
| Item Type: | Article |
|---|---|
| DOI/Identification number: | 10.1021/la0635799 |
| Uncontrolled keywords: | Calcination, Gelation, Nanocomposites, Nanocrystals, Porous materials, Reaction kinetics, Sol-gel process, Synthesis (chemical), Urea, Nanocomposite aerogels, Precursors, Aerogels |
| Subjects: | Q Science > QC Physics > QC176.8.N35 Nanoscience, nanotechnology |
| Institutional Unit: | Schools > School of Engineering, Mathematics and Physics > Physics and Astronomy |
| Former Institutional Unit: |
Divisions > Division of Natural Sciences > Physics and Astronomy
|
| Depositing User: | Anna Corrias |
| Date Deposited: | 16 Dec 2014 15:11 UTC |
| Last Modified: | 20 May 2025 09:35 UTC |
| Resource URI: | https://kar.kent.ac.uk/id/eprint/46175 (The current URI for this page, for reference purposes) |
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https://orcid.org/0000-0002-5190-8196
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