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Iron-Cobalt-Silica aerogel nanocomposite materials

Casula, M.F., Corrias, A., Paschina, G. (2003) Iron-Cobalt-Silica aerogel nanocomposite materials. Journal of Sol-Gel Science and Technology, 26 (1-3). pp. 667-670. ISSN 0928-0707. (doi:10.1023/A:1020761130074) (The full text of this publication is not currently available from this repository. You may be able to access a copy if URLs are provided) (KAR id:46185)

The full text of this publication is not currently available from this repository. You may be able to access a copy if URLs are provided.
Official URL:
http://dx.doi.org/10.1023/A:1020761130074

Abstract

Iron-Cobalt-Silica nanocomposites were prepared in form of aerogels. X-ray diffraction, transmission electron microscopy and N2 physisorption at 77 K were used to investigate the structure, size and dispersion of the nanocrystals and the porous structure in the aerogels and in the final composites. The variation of the supercritical drying conditions gives rise to differences in the morphological features of the aerogels. These differences influence the size of the cobalt oxide nanoparticles in the aerogels. On the other hand, after the reduction treatment the average size of the alloy nanoparticles is the same in all the aerogel nanocomposites. The effect of reduction temperature on alloy formation and particle size is also discussed.

Item Type: Article
DOI/Identification number: 10.1023/A:1020761130074
Uncontrolled keywords: Aerogels, Alloys, Nanocomposites, Drying, Morphology, Nanostructured materials, Nitrogen, Particle size analysis, Reduction, Sorption, Thermal effects, Transmission electron microscopy, X ray diffraction analysis, Physisorption, Aerogels
Subjects: Q Science > QC Physics > QC176.8.N35 Nanoscience, nanotechnology
Divisions: Divisions > Division of Natural Sciences > Physics and Astronomy
Depositing User: Anna Corrias
Date Deposited: 16 Dec 2014 15:10 UTC
Last Modified: 16 Nov 2021 10:18 UTC
Resource URI: https://kar.kent.ac.uk/id/eprint/46185 (The current URI for this page, for reference purposes)
Corrias, A.: https://orcid.org/0000-0002-5190-8196
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