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Optimising selective excitation pulses to maximise saturation transfer difference NMR spectroscopy

Ley, Nathan B., Rowe, Michelle L., Williamson, Richard A., Howard, Mark J. (2014) Optimising selective excitation pulses to maximise saturation transfer difference NMR spectroscopy. RSC Advances, 4 (14). pp. 7347-7351. ISSN 2046-2069. (doi:10.1039/C3RA46246C) (KAR id:44134)

Abstract

A simple method is presented that optimizes the STD NMR Gaussian pulse to deliver significant increases in STD amplification factors with minimal perturbation of the ligand. This approach is practically demonstrated using the wheat-germ agglutinin/N-acetyl-D-glucosamine protein–ligand system.

Item Type: Article
DOI/Identification number: 10.1039/C3RA46246C
Subjects: Q Science > QD Chemistry
Q Science > QH Natural history > QH301 Biology
Divisions: Divisions > Division of Natural Sciences > Biosciences
Depositing User: M.J. Howard
Date Deposited: 06 Nov 2014 17:12 UTC
Last Modified: 16 Feb 2021 12:56 UTC
Resource URI: https://kar.kent.ac.uk/id/eprint/44134 (The current URI for this page, for reference purposes)

University of Kent Author Information

Rowe, Michelle L..

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Williamson, Richard A..

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Howard, Mark J..

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