The 1st structure of a benzo[b][1,4]diazocine

Wallis, J.D. (1992) The 1st structure of a benzo[b][1,4]diazocine. Acta Crystallographica Section C-Crystal Structure Communications, 48 . pp. 897-899. ISSN 0108-2701. (The full text of this publication is not available from this repository)

The full text of this publication is not available from this repository. (Contact us about this Publication)
Official URL
http://dx.doi.org/10.1107/S0108270191012337

Abstract

1-Ethyl-1,2-dihydro-3-methyl-5-phenylbenzo[b][1,4]diazocin-2-one, C19H18N2O, M(r) = 290.4, monoclinic, P2(1)/c, a = 9.714 (3), b = 10.087 (5), c = 15.758 (8) angstrom, beta = 91.67 (4)-degrees, V = 1543.4 angstrom3, Z = 4, D(x) = 1.25 g cm-3, Mo K-alpha radiation, lambda = 0.71069 angstrom, mu = 0.73 cm-1, F(000) = 616, T = 295 K, R = 0.033 for 1806 observed reflections. This novel ring system, prepared by an unprecedented ring expansion of a benzimidazole, has a chiral 'tub' structure.

Item Type: Article
Subjects: Q Science > QD Chemistry
Divisions: Faculties > Science Technology and Medical Studies > School of Biosciences
Depositing User: O.O. Odanye
Date Deposited: 31 Aug 2009 17:42
Last Modified: 31 Aug 2009 17:42
Resource URI: http://kar.kent.ac.uk/id/eprint/22273 (The current URI for this page, for reference purposes)
  • Depositors only (login required):