An NMR apparatus for the measurement of self-diffusion in solids

Gordon, Robert and Strange, John H. and Webber, J. Beau W. (1978) An NMR apparatus for the measurement of self-diffusion in solids. Journal of Physics E: Scientific Instruments, 11 (10). pp. 1051-1055. ISSN 0022-3735. (Access to this publication is restricted)

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http://dx.doi.org/10.1088/0022-3735/11/10/023

Abstract

An apparatus is described which is suitable for measuring self-diffusion coefficients in solids using the nuclear magnetic resonance spin-echo technique employing a pulsed field gradient. The design of the probe arrangement for use at high temperature (to 1300 K) and the electronic circuit to generate the large pulses of magnetic field gradient are described in detail. The apparatus is designed for use with a pulsed NMR spectrometer assuming suitable timing pulses are available. The current switch handles 150 A, and the pulse has a fall time (to 10%) of 50 ps and produces a field gradient of 1.5 T m-1 in a quadrupole coil surrounding the high-temperature probe.

Item Type: Article
Subjects: Q Science > QC Physics
T Technology > TK Electrical engineering. Electronics Nuclear engineering > TK7800 Electronics (see also: telecommunications)
Divisions: Faculties > Science Technology and Medical Studies > School of Physical Sciences > Functional Materials Group
Depositing User: J.B.W. Webber
Date Deposited: 29 Jun 2011 18:00
Last Modified: 07 Jul 2014 13:52
Resource URI: http://kar.kent.ac.uk/id/eprint/13446 (The current URI for this page, for reference purposes)
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